Time and Temperature for Shatter

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October420

the King of October
Joined
Aug 31, 2014
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Hey folks, trying to work out my technique for Shatter. I've included a picture of my last run, this is actually my second attempt at it. So I blasted fresh frozen bud into a Pyrex dish, placed the dish into a pan of hot water to boil off much of the butane. Placed the remaining oil into a vacuum chamber and purged 20 hours, 12 of the 20 hours I set the temperature at 105°F. Although I'm happy with the purity and quality of my product, it's not shatter. I believe it has to do with the time and temperature I purged at. Looking for suggestions on achieving shatter.

Thanks
 

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